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"I asked, 'Are you sure you don't have anything else?' He started singing and playing 'Everything is alright, uptight.' That was as much as he had. As Wonder presented his ideas, finished or not, "he went through everything," remembered Moy. Nelson George, in Where Did Our Love Go? The Rise and Fall of the Motown Sound, recorded that Wonder had also sought something based on the driving beat of the Rolling Stones' " (I Can't Get No) Satisfaction", after playing several dates with the Stones on tour and being impressed with the British band. In addition, Wonder's voice had begun to change, and Motown CEO Berry Gordy was worried that he would no longer be a commercially viable artist.Īs it turned out, however, producer Clarence Paul found it easier to work with Wonder's now-mature tenor voice, and Sylvia Moy and Henry Cosby set about writing a new song for the artist, based upon an instrumental riff Wonder had devised. And despite receiving a modicum of chart success, the then 15-year-old Wonder was in danger of being let go. Aside from the US number-one " Fingertips" (1963), only two of Wonder's singles, "Workout, Stevie, Workout" (1963) and " Hey Harmonica Man" (1964) had both peaked inside of the top forty of the US Billboard Hot 100 chart, peaking at #33 and #29 on that chart respectively. The single was a watershed in Wonder's career for several reasons. ![]() THE SYNTHESIS OF CURCUMINE ANALOGUE MONOCETONE FROM CINAMALDEHYDE AND ITS ACTIVITY TEST AS α-GLUCOCYDE ENZYME INHIBITOR Hasil uji inhibisi terhadap enzim α-glukosidase mengindikasi bahwa analog kurkumin memiliki aktivitas antidiabetik dan cukup berpotensi untuk menginhibisi enzim α-glukosidase dengan persentase inhibisi sebesar 70,71%. Hasil berupa padatan berwana kuning dengan titik leleh sebesar 196,20–200,10 ☌. Hasil penelitian menunjukkan bahwa analog kurkumin monoketon hasil sintesis diperoleh rendemen sebesar 72,15%. ![]() Tahap selanjutnya analog kurkumin hasil sintesis diuji aktivitasnya sebagai inhibitor enzim α-glukosidase. Senyawa hasil sintesis dianalisis strukturnya menggunakan FTIR, direct inlet-MS, 1H- dan 13C-NMR. Sintesis tersebut dilakukan dalam kondisi basa KOH dengan pengadukan pada suhu 52 ☌ selama 50 menit. Tahapan awal penelitian ini yaitu analog kurkumin (2 E,5 E)-2,5-bis(( E)-3-fenilalilidin) siklopentanon disintesis dengan mereaksikan sinamaldehid dan monoketon siklopentanon dalam pelarut etanol. Pengujian aktivitas antidiabetes senyawa analog kurkumin dilakukan melalui inhibisi enzim α-glukosidase yang diisolasi dari beras lapuk ( Oryza sativa). Tahap sintesis melibatkan reaksi kondensasi aldol silang Claisen-Schmidt dengan variasi keton sehingga dihasilkan senyawa analog kurkumin monoketon. ![]() Telah dilakukan sintesis analog kurkumin monoketon sebagai senyawa target yang berbahan dasar sinamaldehida dan uji aktivitasnya sebagai inhibitor enzim α-glukosidase. 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